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  • BSI
    BS EN ISO 17294-2:2016 Water quality. Application of inductively coupled plasma mass spectrometry (ICP-MS) - Determination of selected elements including uranium isotopes
    Edition: 2016
    $418.55
    / user per year

Description of BS EN ISO 17294-2:2016 2016

This part of ISO 17294 specifies a method for the determination of the elements aluminium, antimony, arsenic, barium, beryllium, bismuth, boron, cadmium, caesium, calcium, cerium, chromium, cobalt, copper, dysprosium, erbium, gadolinium, gallium, germanium, gold, hafnium, holmium, indium, iridium, iron, lanthanum, lead, lithium, lutetium, magnesium, manganese, mercury, molybdenum, neodymium, nickel, palladium, phosphorus, platinum, potassium, praseodymium, rubidium, rhenium, rhodium, ruthenium, samarium, scandium, selenium, silver, sodium, strontium, terbium, tellurium, thorium, thallium, thulium, tin, tungsten, uranium and its isotopes, vanadium, yttrium, ytterbium, zinc and zirconium in water (for example, drinking water, surface water, ground water, waste water and eluates).

Taking into account the specific and additionally occurring interferences, these elements can also be determined in digests of water, sludges and sediments (for example, digests of water as described in ISO 15587‑1 or ISO 15587‑2 ).

The working range depends on the matrix and the interferences encountered. In drinking water and relatively unpolluted waters, the limit of quantification ( xLQ) lies between 0,002 µg/l and 1,0 µg/l for most elements (see Table 1). The working range typically covers concentrations between several pg/l and mg/l depending on the element and pre-defined requirements.

The quantification limits of most elements are affected by blank contamination and depend predominantly on the laboratory air-handling facilities available on the purity of reagents and the cleanliness of glassware.

The lower limit of quantification is higher in cases where the determination suffers from interferences (see Clause 5) or memory effects (see ISO 17294‑1:2004 , 8.2).

Table 1
Lower limits of quantification ( xLQ) for unpolluted water
Element Isotope often used Limit of quantification a

µg/l

 Element Isotope often used Limit of quantification a

µg/l

 Element Isotope often used Limit of quantification a

µg/l
Ag 107Ag 0,5 Hf 178Hf 0,1 Ru 102Ru 0,1
109Ag 0,5 Hg 202Hg 0,05 Sb 121Sb 0,2
Al 27Al 1 Ho 165Ho 0,1 123Sb 0,2
As 75As c 0,1 In 115In 0,1 Sc 45Sc 5
Au 197Au 0,5 Ir 193Ir 0,1 Se 77Se c 1
B 10B 1 K 39K C 5 78Se c 0,1
11B 1 La 139La 0,1 82Se 1
Ba 137Ba 3 Li 6Li 10 Sm 147Sm 0,1
138Ba 0,5 7Li 1 Sn 118Sn 1
Be 9Be 0,1 Lu 175Lu 0,1 120Sn 1
Bi 209Bi 0,5 Mg 24Mg 1 Sr 86Sr 0,5
Ca 43Ca 100 25Mg 10 88Sr 0,3
44Ca 50 Mn 55Mn 0,1 Tb 159Tb 0,1
40Ca 10 Mo 95Mo 0,5 Te 126Te 2
Cd 111Cd 0,1 98Mo 0,3 Th 232Th 0,1
114Cd 0,5 Na 23Na 10 Tl 203Tl 0,2
Ce 140Ce 0,1 Nd 146Nd 0,1 205Tl 0,1
Co 59Co 0,2 Ni 58Nic 0,1 Tm 169Tm 0,1
Cr 52Crc 0,1 60Nic 0,1 U 238U 0,1
53Cr 5 P 31P 5 235U 10-4
Cs 133Cs 0,1 Pb 206Pb b 0,2 234U 10-5
Cu 63Cu 0,1 207Pb b 0,2 V 51V c 0,1
65Cu 0,1 208Pb b 0,1 W 182W 0,3
Dy 163Dy 0,1 Pd 108Pd 0,5 184W 0,3
Er 166Er 0,1 Pr 141Pr 0,1 Y 89Y 0,1
Fe 56Fe c 5 Pt 195Pt 0,5 Yb 172Yb 0,2
Ga 69Ga 0,3 Rb 85Rb 0,1 174Yb 0,2
71Ga 0,3 Re 185Re 0,1 Zn 64Zn 1
Gd 157Gd 0,1 187Re 0,1 66Zn 1
158Gd 0,1 Rh 103Rh 0,1 68Zn 1
Ge 74Ge 0,3 Ru 101Ru 0,2 Zr 90Zr 0,2
a

Depending on the instrumentation, significantly lower limits can be achieved.

b

In order to avoid incorrect results due to the varying isotop ratios in the environment, the signal intensities of 206Pb, 207Pb and 208Pb shall be added.

c

In order to reach these limits, depending on interferences, the use of a collision/reaction cell is recommended



Standard NumberBS EN ISO 17294-2:2016
TitleWater quality. Application of inductively coupled plasma mass spectrometry (ICP-MS) - Determination of selected elements including uranium isotopes
StatusWithdrawn
Publication Date2016-08-31
Withdrawn Date2023-11-01
ReplacesBS EN ISO 17294-2:2004
Replaced ByBS EN ISO 17294-2:2023
Identical National Standard OfEN ISO 17294-2 (ISO 17294-2:2016) AS, ISO 17294-2:2016
DescriptorsGallium, Ground water, Nickel, Molybdenum, Selenium, Platinum, Mass spectrometry, Water pollution, Tin inorganic compounds, Rubidium, Lithium, Tellurium, Hafnium, Lead, Manganese, Interferences (chemical), Sodium, Barium, Thorium, Zirconium, Uranium, Lanthanides, Ruthenium, Indium, Determination of content, Rhodium, Calcium, Water testing, Quality, Cadmium, Iridium, Potable water, Silver, Vanadium, Water, Arsenic, Antimony, Potassium, Copper, Sludge, Tungsten, Rhenium, Germanium, Phosphorus, Scandium, Metals, Strontium, Gold, Spectroscopy, Chemical analysis and testing, Boron, Caesium, Thallium, Bismuth, Yttrium, Chromium, Cobalt, Palladium, Beryllium, Zinc, Surface water, Magnesium, Aluminium
ICS13.060.50 Examination of water for chemical substances
CommitteeEH/3/2
ISBN978 0 580 82291 9
PublisherBSI
Pages42

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About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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