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eLibrary > PD CEN/TS 17847:2022 Characterization of waste. Determination of selected low boiling point alcohols using gas chromatography with flame ionization detection after static head-space extraction (HS-GC-FID) >

PD CEN/TS 17847:2022 Characterization of waste. Determination of selected low boiling point alcohols using gas chromatography with flame ionization detection after static head-space extraction (HS-GC-FID), 2022

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PD CEN/TS 17847:2022 Characterization of waste. Determination of selected low boiling point alcohols using gas chromatography with flame ionization detection after static head-space extraction (HS-GC-FID), 2022

National foreword
European foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Interferences [Go to Page]
5.1 Interferences with sampling and extraction
5.2 Interferences with GC
6 Apparatus and reagents [Go to Page]
6.1 Apparatus [Go to Page]
6.1.3 Flame ionization detector
6.1.6 Automatic syringe or bottle top dispenser
6.2 Reagents [Go to Page]
6.2.1 Ultra pure water
6.2.3 Dimethylformamide, C3H7NO
6.2.4 Sodium chloride, NaCl
6.2.7 Stock solutions
6.3 Sampling, storage and pretreatment [Go to Page]
6.3.1 Sampling
6.3.2 Storage
6.3.3 Preatreatment
7 Procedure [Go to Page]
7.1 Determination of dry matter via water content for pasty waste
7.2 Calibration
7.3 Mass of sample
7.4 Analysis [Go to Page]
7.4.1 Identification of selected alcohols by retention times on the chromatogram obtained by GC-FID
7.4.2 Confirmation criteria for the identification of selected alcohol
7.4.3 Procedure
8 Calculation [Go to Page]
8.1 Calibration function
8.2 Calculation of selected alcohol concentration in the sample
9 Expression of results
10 Test report
Annex A (informative) Examples of gas chromatographic conditions
Bibliography [Go to Page]

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PD CEN/TS 17847:2022 Characterization of waste. Determination of selected low boiling point alcohols using gas chromatography with flame ionization detection after static head-space extraction (HS-GC-FID), 2022

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