ASTM C114-11b
Historical Standard: ASTM C114-11b Standard Test Methods for Chemical Analysis of Hydraulic Cement
SUPERSEDED (see Active link, below)
ASTM C114
1. Scope
1.1 These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 4. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific analytes and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method.
1.2 Contents:
| Section |
Subject |
| 2 | Referenced Documents |
| 4 | Description of Referee Analyses |
| 4.1 | Referee Analyses |
| 5 | Qualification for Different Analyses |
| 5.1 | Certified Reference Materials |
| 5.2 | Requirements for Qualification Testing |
| 5.3 | Alternative Analyses |
| 5.4 | Performance Requirements for Rapid Test Methods |
| 6 | General |
| 6.1 | Interferences and Limitations |
| 6.2 | Apparatus and Materials |
| 6.3 | Reagents |
| 6.4 | Sample Preparation |
| 6.5 | General Procedures |
| 6.6 | Recommended Order for Reporting Analyses |
|
Reference Test Methods |
|
| 7 | Insoluble Residue |
| 8 | Silicon Dioxide |
| 8.2 | Cements with Insoluble Residue Less Than 1 % |
| 8.3 | Cements with Insoluble Residue Greater Than 1 % |
| 9 | Ammonium Hydroxide Group |
| 10 | Ferric Oxide |
| 11 | Phosphorus Pentoxide |
| 12 | Titanium Dioxide |
| 13 | Zinc Oxide |
| 14 | Aluminum Oxide |
| 15 | Calcium Oxide |
| 16 | Magnesium Oxide |
| 17 | Sulfur |
| 17.1 | Sulfur Trioxide |
| 17.2 | Sulfide |
| 18 | Loss On Ignition |
| 18.1 | Portland Cement |
| 18.2 | Portland Blast-Furnace Slag Cement and Slag Cement |
| 19 | Sodium and Potassium Oxides |
| 19.1 | Total Alkalis |
| 19.2 | Water-Soluble Alkalis |
| 20 | Manganic Oxide |
| 21 | Chloride |
| 22 | Chloroform-Soluble Organic Substances |
|
Alternative Test Methods |
|
| 23 | Calcium Oxide |
| 24 | Carbon Dioxide |
| 25 | Magnesium Oxide |
| 26 | Loss on Ignition |
| 26.1 | Portland Blast-Furnace Slag Cement and Slag Cement |
| 27 | Titanium Dioxide |
| 28 | Phosphorus Pentoxide |
| 29 | Manganic Oxide |
| 30 | Free Calcium Oxide |
| Appendices |
Title |
| Appendix X1 |
Example of Determination of Equivalence Point for the Chloride Determination |
| Appendix X2 | CO 2 Determinations in Hydraulic Cements |
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 8.3.2.1 and 16.4.1 for specific caution statements.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
C25 Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime
D1193 Specification for Reagent Water
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E275 Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers
E350 Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
E617 Specification for Laboratory Weights and Precision Mass Standards
E832 Specification for Laboratory Filter Papers
Keywords
chemical analysis; compositional analysis; hydraulic cements;
ICS Code
ICS Number Code 91.100.10 (Cement. Gypsum. Lime. Mortar)
DOI: 10.1520/C0114-11B
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