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  • ASTM
    C1647-13 Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials
    Edition: 2013
    $91.10
    Unlimited Users per year

Description of ASTM-C1647 2013

ASTM C1647 - 13

Standard Practice for Removal of Uranium or Plutonium, or both, for Impurity Assay in Uranium or Plutonium Materials

Active Standard ASTM C1647 | Developed by Subcommittee: C26.05

Book of Standards Volume: 12.01




ASTM C1647

Significance and Use

5.1 This practice can be used to separate uranium or plutonium, or both, prior to the impurity analysis by various techniques. The removal of uranium and plutonium prior to quantification can improve the detection limits by minimizing the signal suppression caused by uranium or plutonium when using ICP techniques. Detection limits of ~110 part-per-billion (PPB) may be obtainable by matrix removal. Also, removal of the uranium and plutonium may allow the impurities analysis to be performed on a non-glove box enclosed instrument.

5.2 Other test methods exist to determine impurities in uranium or plutonium. Test Method C1517 is able to determine many impurities in uranium at detection levels of ~110 part-per-million (ppm) by DC-Arc Spectrometry. Test Method C1287 is able to determine impurities in uranium at detection levels of ~100 ppb by ICP-MS. Test Method C1432 provides an alternative technique to remove plutonium by ion exchange prior to analysis of the impurities by ICP-AES.

5.3 This practice can be used to demonstrate compliance with nuclear fuel specifications, for example, Specifications C753 , C757 , C776 , C787 , C788 , and C996 .

1. Scope

1.1 This practice covers instructions for using an extraction chromatography column method for the removal of plutonium or uranium, or both, from liquid or digested oxides or metals prior to impurity measurements. Quantification of impurities can be made by techniques such as inductively coupled plasma mass spectrometry (ICP-MS), inductively coupled plasma atomic emission spectrometry (ICP-AES) or atomic absorption spectrometry (AAS.)

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

C753 Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder

C757 Specification for Nuclear-Grade Plutonium Dioxide Powder, Sinterable

C776 Specification for Sintered Uranium Dioxide Pellets

C787 Specification for Uranium Hexafluoride for Enrichment

C788 Specification for Nuclear-Grade Uranyl Nitrate Solution or Crystals

C859 Terminology Relating to Nuclear Materials

C996 Specification for Uranium Hexafluoride Enriched to Less Than 5 % 235U

C1168 Practice for Preparation and Dissolution of Plutonium Materials for Analysis

C1287 Test Method for Determination of Impurities in Nuclear Grade Uranium Compounds by Inductively Coupled Plasma Mass Spectrometry

C1347 Practice for Preparation and Dissolution of Uranium Materials for Analysis

C1432 Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis

C1517 Test Method for Determination of Metallic Impurities in Uranium Metal or Compounds by DC-Arc Emission Spectroscopy

D1193 Specification for Reagent Water


Keywords

AAS; extraction chromatography; ICP-AES; ICP-MS; impurities; plutonium; resin; separation; uranium;


ICS Code

ICS Number Code 71.040.50 (Physicochemical methods of analysis)


DOI: 10.1520/C1647-13

ASTM International is a member of CrossRef.

ASTM C1647

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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