1. Scope

1.1 This practice covers methods for withdrawing representative sample(s) of uranium hexafluoride (UF ₆ ) during a transfer occurring in the gas phase. Such transfer in the gas phase can take place from a mother cylinder, for example in an autoclave to a receiving cylinder. It can also occur during the filling in the gas phase of a cylinder during a continuous production process, for example centrifuge enrichment facility or the distillation column in a conversion facility. Such sample(s) may be used for determining compliance with the applicable commercial specification, for example Specification C 996 or Specification C 787 .

1.2 Since UF ₆ sampling is taken during the filling process, this practice does not address any special additional arrangements that may be agreed upon between the buyer and the seller when the sampled bulk material is being added to residues already present in a container ( heels recycle ). Such arrangements will be based on QA procedures such as traceability of cylinder origin (to prevent for example contamination with irradiated material).

1.3 If the receiving cylinder is purged after filling and sampling, special verifications must be performed by the user to verify the representativity of the sample(s). It is then expected that the results found on volatile impurities with gas phase sampling may be conservative.

1.4 This practice is only applicable when the transfer occurs in the gas phase. When the transfer is performed in the liquid phase, Practice C 1052 should apply. This practice does not apply to gas sampling after the cylinder has been filled since the sample taken will not be representative of the cylinder.

1.5 The scope of this practice does not include provisions for preventing criticality incidents.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

C761 Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride

C787 Specification for Uranium Hexafluoride for Enrichment

C996 Specification for Uranium Hexafluoride Enriched to Less Than 5 % 235U

C1052 Practice for Bulk Sampling of Liquid Uranium Hexafluoride

Other Document

Keywords

bulk sampling; nuclear material; uranium hexafluoride;

ICS Code

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)

DOI: 10.1520/C1703-08

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