1. Scope

1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade mixed oxides, (U, Pu)O 2 , powders and pellets to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safeguard and safety precaution statements, see Sections 11, 20, 64, and 112 and 102.6.1.)

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

C697 Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets

C833 Specification for Sintered (Uranium-Plutonium) Dioxide Pellets

C852 Guide for Design Criteria for Plutonium Gloveboxes

C1008 Specification for Sintered (Uranium-Plutonium) Dioxide Pellets--Fast Reactor Fuel

C1009 Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry

C1068 Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry

C1108 Test Method for Plutonium by Controlled-Potential Coulometry

C1128 Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials

C1156 Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials

C1165 Test Method for Determining Plutonium by Controlled-Potential Coulometry in H2SO4 at a Platinum Working Electrode

C1168 Practice for Preparation and Dissolution of Plutonium Materials for Analysis

C1204 Test Method for Uranium in Presence of Plutonium by Iron(II) Reduction in Phosphoric Acid Followed by Chromium(VI) Titration

C1206 Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration

C1210 Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry

C1268 Test Method for Quantitative Determination of Americium 241 in Plutonium by Gamma-Ray Spectrometry

C1297 Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials

C1415 Test Method for 238Pu Isotopic Abundance By Alpha Spectrometry

C1432 Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis

D1193 Specification for Reagent Water

E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry

E115 Practice for Photographic Processing in Optical Emission Spectrographic Analysis

E116 Practice for Photographic Photometry in Spectrochemical Analysis

Keywords

Carbon content--nuclear materials; Chloride analysis--nuclear applications; Fluoride content; Isotopic analysis; Mass spectrometry--nuclear materials/applications; Mixed oxides (MOX); Moisture analysis--nuclear materials; Nitrogen content--nuclear materials; Plutonium--isotopic analysis; Rare earth content; Spectrochemical analysis; Sulfur--nuclear materials; Trace elements--spectrochemical analysis; Tungsten content; Uranium content; Volatile matter content--nuclear materials;

ICS Code

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)

DOI: 10.1520/C0698-04

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