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  • ASTM
    C759-18 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions
    Edition: 2018
    $94.85
    Unlimited Users per year

Description of ASTM-C759 2018

ASTM C759-18

Active Standard: Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions




ASTM C759

Scope

1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium nitrate solutions to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

 

Sections

 

Plutonium by Controlled-Potential Coulometry

2

Plutonium by Amperometric Titration with Iron(II)

2

Plutonium by Diode Array Spectrophotometry

 

Free Acid by Titration in an Oxalate Solution

8 to 15

Free Acid by Iodate Precipitation-Potentiometric Titration
  Test Method

16 to 22

Uranium by Arsenazo I Spectrophotometric Test Method

23 to 33

Thorium by Thorin Spectrophotometric Test Method

34 to 42

Iron by 1,10-Phenanthroline Spectrophotometric Test Method

43 to 50

Impurities by ICP-AES

 

Chloride by Thiocyanate Spectrophotometric Test Method

51 to 58

Fluoride by Distillation-Spectrophotometric Test Method

59 to 66

Sulfate by Barium Sulfate Turbidimetric Test Method

67 to 74

Isotopic Composition by Mass Spectrometry

75 to 76

Plutonium-238 Isotopic Abundance by Alpha Spectrometry

 

Americium-241 by Extraction and Gamma Counting

77 to 85

Americium-241 by Gamma Counting

86 to 94

Gamma-Emitting Fission Products, Uranium, and Thorium by Gamma-Ray Spectroscopy

94 to 102

Rare Earths by Copper Spark Spectrochemical Test Method

103 to 105

Tungsten, Niobium (Columbium), and Tantalum by Spectro-
 chemical Test Method

106 to 114

Sample Preparation for Spectrographic Analysis for General
 Impurities

115 to 118

1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety hazard statements, see Section 6.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

impurity content; isotopic composition; plutonium content; plutonium nitrate;


ICS Code

ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)


DOI: 10.1520/C0759-18

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2004
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2010
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2018
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Model Standard
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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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