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  • ASTM
    D128-98(2003)e1 Standard Test Methods for Analysis of Lubricating Grease
    Edition: 2003
    $113.57
    Unlimited Users per year

Description of ASTM-D128 2003

ASTM D128-98-e1-Reapproved2003

Historical Standard: Standard Test Methods for Analysis of Lubricating Grease




ASTM D128

Scope

1.1 These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles.

Note 1—Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires.

1.2 A supplementary test method is provided in Appencix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions.

1.3 These test methods appear in the following order:

Sections
Ash Determination 7-11
Insolubles, Soap, Fat, Petroleum Oil,and Unsaponifiable Matter 12-20
Free Alkali and Free Acid 21-23
Water 24
Glycerin (Quantitative) 25-29

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices, and determine the applicability of regulatory limitations prior to use.

1.5 The values stated in SI units are to be regarded as the standard.


Keywords

analysis; extraction; fat content; fluid content; free alkali content; free fatty acid content; glycerin content; insolubles content; lubricating grease; petroleum oil content; soap content; Soxhlet apparatus; thickener content; water content


ICS Code

ICS Number Code n/a


DOI: 10.1520/D0128-98R03E01

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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