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Description of ASTM-D3328 2013ASTM D3328 - 06(2013)Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas ChromatographyActive Standard ASTM D3328 | Developed by Subcommittee: D19.06 Book of Standards Volume: 11.02 ASTM D3328Significance and Use 4.1 Identification of a recovered oil is determined by comparison with known oils, selected because of their possible relationship to the particular recovered oil. The known oils are collected from suspected sources. Samples of such known oils must be collected and submitted along with the unknown for analysis. At present, identification of the source of an unknown oil by itself cannot be made (for example, from a library of known oils). 4.2 The use of a flame-photometric detector in addition to the flame-ionization detector provides a second, independent profile of the same oil, that is, significantly more information is available from a single analysis with dual detection. 4.3 Many close similarities (within uncertainties of sampling and analysis) will be needed to establish identity beyond a reasonable doubt. The analyses described will distinguish many, but not all samples. For cases in which this method does not clearly identify a pair of samples, and for important cases where additional comparisons are needed to strengthen conclusions, other analyses will be required (refer to Practice D3415 ). In particular, Practice D5739 is useful for such cases. 1. Scope 1.1 This test method covers the comparison of petroleum oils recovered from water or beaches with oils from suspect sources by means of gas chromatography ( 1 , 2 , 3 ) . 2 Such oils include distillate fuel, lubricating oil, and crude oil. The test method described is for capillary column analyses using either single detection (flame ionization) or dual detection (flame ionization and flame photometric) for sulfur containing species. 1.2 This test method provides high resolution for critical examination of fine structure that is resistant to weathering. The flame-photometric detection for sulfur components is an adjunct, not a substitute, for flame-ionization detection in the identification of waterborne petroleum oils ( 4- 12 ) . For this reason, flame photometric detection is optional. 1.3 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM Standards D1129 Terminology Relating to Water D1193 Specification for Reagent Water D2549 Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography D3325 Practice for Preservation of Waterborne Oil Samples D3326 Practice for Preparation of Samples for Identification of Waterborne Oils D3415 Practice for Identification of Waterborne Oils D4489 Practices for Sampling of Waterborne Oils D5739 Practice for Oil Spill Source Identification by Gas Chromatography and Positive Ion Electron Impact Low Resolution Mass Spectrometry E355 Practice for Gas Chromatography Terms and Relationships Keywords gas chromotograph; oil analysis; oil identification; spilled oils; waterborne oils; ICS Code ICS Number Code 75.080 (Petroleum products in general) DOI: 10.1520/D3328-06R13 ASTM International is a member of CrossRef. ASTM D3328This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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