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Description of ASTM-D3452 2017ASTM D3452-06-Reapproved2017Historical Standard: Standard Practice for Rubber—Identification by Pyrolysis-Gas ChromatographyASTM D3452Scope 1.1 This practice covers the identification of polymers in raw rubbers, and cured and uncured compounds, based on a single polymer, by the gas chromatographic patterns of their pyrolysis products (pyrograms). Implementation of this guide presupposes a working knowledge of the principles and techniques of gas chromatography, sufficient to carry out this practice and to interpret the results correctly.2 1.2 This practice will identify the following polymers: 1.2.1 Polyisoprene of natural or synthetic origin, 1.2.2 Butadiene-styrene copolymers, 1.2.3 Polybutadiene, 1.2.4 Polychloroprene, 1.2.5 Butadiene-acrylonitrile copolymers, 1.2.6 Ethylene-propylene copolymers and related terpolymers, and 1.2.7 Isobutene-isoprene copolymers. 1.3 This practice will not differentiate the following polymers: 1.3.1 Natural polyisoprene from synthetic polyisoprene. 1.3.2 Butadiene-styrene copolymers produced by solution and emulsion polymerization. It is sometimes possible to distinguish butadiene-styrene copolymers containing different amounts of styrene as well as random polymers from block polymers. 1.3.3 Polybutadiene with different microstructures. 1.3.4 Different types of polychloroprenes. 1.3.5 Butadiene-acrylonitrile copolymers with different monomer ratios. 1.3.6 Ethylene-propylene copolymers with different monomer ratios, as well as the copolymers from the related terpolymers. 1.3.7 Isobutene-isoprene copolymers (butyl rubbers) from halogenated butyl rubbers. 1.3.8 Polyisoprene containing different amounts of cis-trans isomers. 1.3.9 The practice does not identify ebonite or hard rubbers. 1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. Keywords GC; gas chromatography; pyrogram; pyrolysis; rubber composition; rubber identification; ICS Code ICS Number Code 83.060 (Rubber) DOI: 10.1520/D3452-06R17 This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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