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  • ASTM
    D3545-06(2012) Standard Test Method for Alcohol Content and Purity of Acetate Esters by Gas Chromatography
    Edition: 2012
    $113.57
    Unlimited Users per year

Description of ASTM-D3545 2012

ASTM D3545 - 06(2012)

Standard Test Method for Alcohol Content and Purity of Acetate Esters by Gas Chromatography

Active Standard ASTM D3545 | Developed by Subcommittee: D01.35

Book of Standards Volume: 06.04




ASTM D3545

Significance and Use

4.1 This test method is useful for identifying and for determining the quantity of various impurities in acetate esters.

4.2 Total purity of the acetate esters must be determined by use of other appropriate ASTM procedures with this test method.

1. Scope

1.1 This test method covers the determination by gas chromatography of the ester content and the corresponding alcohol content of acetate esters. This test method has been applied to ethyl, n -propyl, isopropyl, n -butyl, isobutyl, and 2-ethoxyethyl acetates.

1.2 Water, and in some cases acetic acid, cannot be determined by this test method and must be measured by other appropriate ASTM procedures and the results used to normalize the chromatographic value.

1.3 For purposes of determining conformance of an observed or a calculated value using this test method to relevant specifications, test result(s) shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29 .

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for material listed in this specification.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D1364 Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)

D1613 Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products

D2593 Test Method for Butadiene Purity and Hydrocarbon Impurities by Gas Chromatography

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E180 Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Specialty Chemicals

E260 Practice for Packed Column Gas Chromatography


Keywords

acetate esters; alcohol content; purity;


ICS Code

ICS Number Code 87.060.30 (Solvents)


DOI: 10.1520/D3545-06R12

ASTM International is a member of CrossRef.

ASTM D3545

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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