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Description of ASTM-D3685/D3685M 2013ASTM D3685/D3685M-13Historical Standard: Standard Test Methods for Sampling and Determination of Particulate Matter in Stack GasesASTM D3685/D3685MScope 1.1 These test methods describe procedures to determine the mass emission rates of particulate matter and collected residue in gaseous streams by in-stack test methods (Test Method A) or out-of-stack test methods (Test Method B). 1.2 These test methods are suitable for measuring particulate matter and collected residue concentrations. 1.3 These test methods include a description of equipment and procedures to be used for obtaining samples from effluent ducts and stacks, a description of equipment and procedures for laboratory analysis, and a description of procedures for calculating results. 1.4 These test methods are applicable for sampling particulate matter and collected residue in wet (Test Method A or B) or dry (Test Method A) streams before and after particulate matter control equipment, and for determination of control device particulate matter collection efficiency. 1.5 These test methods are also applicable for determining compliance with regulations and statutes limiting particulate matter existing in stack gases when approved by federal or state agencies. 1.6 The particulate matter and collected residue samples collected by these test methods may be used for subsequent size and chemical analysis. 1.7 These test methods describe the instrumentation, equipment, and operational procedures, including site selection, necessary for sampling and determination of particulate mass emissions. These test methods also include procedures for collection and gravimetric determination of residues collected in an impinger-condenser train. The sampling and analysis of particulate matter may be performed independently or simultaneously with the determination of collected residue. 1.8 These test methods provide for the use of optional filter designs and filter material as necessary to accommodate the wide range of particulate matter loadings to which the test methods are applicable. 1.9 Stack temperatures limitation for Test Method A is approximately 400°C (752°F) and for Test Method B is 815°C (1500°F). 1.10 A known limitation of these test methods concerns the use of collected residue data. Since some collected residues can be formed in the sample train by chemical reaction in addition to condensation, these data should not be used without prior characterization (see 4.4.1). 1.10.1 A second limitation concerns the use of the test methods for sampling gas streams containing fluoride, or ammonia or calcium compounds in the presence of sulfur dioxide and other reactive species having the potential to react within the sample train. 1.10.2 A suspected but unverified limitation of these test methods concerns the possible vaporization and loss of collected particulate organic matter during a sampling run. 1.11 The values stated in either SI units or inch-pound units are to be regarded separately as standard within the text. The inch-pound units are shown in parentheses. The values stated in each system are not exact equivalents; therefore each system shall be used independently of the other. Combining values from the two systems may result in nonconformance to this standard. 1.12 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Keywords EPA Method 5; EPA Method 17; isokinetic sampling; particulate matter; particulate matter sampling; stack sampling ICS Code ICS Number Code 13.040.40 (Stationary source emissions) DOI: 10.1520/D3685_D3685M-13 The following editions for this book are also available...This book also exists in the following packages...Subscription InformationMADCAD.com ASTM Standards subscriptions are annual and access is unlimited concurrency based (number of people that can access the subscription at any given time) from single office location. For pricing on multiple office location ASTM Standards Subscriptions, please contact us at info@madcad.com or +1 800.798.9296.
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About ASTMASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide. |
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