ASTM D4590-00
Historical Standard: ASTM D4590-00 Standard Test Method for Colorimetric Determination of p-tert -Butylcatechol In Styrene Monomer or AMS (alpha-Methylstyrene) by Spectrophotometry
SUPERSEDED (see Active link, below)
ASTM D4590
1. Scope
1.1 This test method is applicable to the determination of residual 4-tertiary-butylcatechol (TBC) in styrene monomer or AMS in the 1 to 100 ppm range. Any other compound known to produce color when contacted with aqueous sodium hydroxide solution will interfere. It may be compensated for by including it in the preparation of the standard solutions, if its identity and concentration in the sample are known.
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off 'to the nearest unit' in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific statements on hazards, see Section 7.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1193 Specification for Reagent Water
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D4790 Terminology of Aromatic Hydrocarbons and Related Chemicals
D6809 Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
Other Document
OSHARegulations,29CF paragraphs 1910.1000 and 1910.1200 Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://www.access.gpo.gov.Keywords
alpha-methylstyrene; AMS; para-tertiary butyl catechol; PTBC; styrene, inhibitor content; styrene, TBC content; TBC in styrene;
ICS Code
ICS Number Code 17.180.20 (Colours and measurement of light); 71.080.60 (Alcohols. Ethers)
DOI: 10.1520/D4590-00
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