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  • ASTM
    D5198-17(2024) Standard Practice for Nitric Acid Digestion of Solid Waste
    Edition: 2024
    $76.13
    Unlimited Users per year

Description of ASTM-D5198 2024

ASTM D5198-17-Reapproved2024

Active Standard: Standard Practice for Nitric Acid Digestion of Solid Waste




ASTM D5198

Scope

1.1 This practice describes the partial digestion of solid waste using nitric acid for the subsequent determination of the total recoverable content of inorganic constituents.

1.2 This practice is to be used when the concentrations of total recoverable elements are to be determined from a waste sample. Total recoverable elements are often not equivalent to total elemental content, because of the solubility of the speciated forms of the element in the sample matrix. Recovery from refractory sample matrices, such as soils, is usually significantly less than total concentrations of the elements present.

Note 1: This practice has been used successfully for oily sludges and a municipal digested sludge standard (Environmental Protection Agency (EPA) Sample No. 397). The practice may be applicable to some elements not listed above, such as arsenic, barium, selenium, cobalt, magnesium, and calcium. Refractory elements such as silicon, silver, and titanium, as well as organo-mercury, are not solubilized by this practice.

1.3 This practice has been divided into two methods, A and B, with Method A utilizing an electric hot plate and Method B utilizing an electric digestion block.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


Keywords

digestion; nitric acid; waste;


ICS Code

ICS Number Code 13.030.10 (Solid wastes)


DOI: 10.1520/D5198-17R24

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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