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  • ASTM
    D5351-93(2009) Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Extraction Titration, Test Method B
    Edition: 2009
    $91.10
    Unlimited Users per year

Description of ASTM-D5351 2009

ASTM D5351 - 93(2009)

Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Extraction Titration, Test Method B

Active Standard ASTM D5351 | Developed by Subcommittee: D31.08

Book of Standards Volume: 15.04




ASTM D5351

Significance and Use

This test method is intended for the determination of organically combined sulfuric anhydride in sulfated oils.

1. Scope

1.1 This test method covers the determination of the organically combined sulfuric anhydride existing in a sample of sulfated oil by extracting the undecomposed sulfated fat and other fatty matter over an acidulated, concentrated salt solution, boiling the residue with sulfuric acid after evaporating the solvent, and titrating the products of reaction. This test method is applicable only to sulfated oils that split off their combined SO 3 upon boiling with mineral acids, including samples containing sodium acetate or other compounds that cannot be accurately titrated in water solution with methyl orange as the indicator. This test method was derived from Test Methods D 500 , Sections 20 through 24, and ALCA Method H-43.

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D500 Test Methods of Chemical Analysis of Sulfonated and Sulfated Oils


Keywords

extraction; leather; sulfated oils; sulfuric anhydride; titration; Leather cleaning/softening compounds; Organically combined sulfuric anhydride; Sulfonated and sulfated oils; Sulfuric anhydride; Titration;


ICS Code

ICS Number Code 71.080.01 (Organic chemicals in general)


DOI: 10.1520/D5351-93R09

ASTM International is a member of CrossRef.

ASTM D5351

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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