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  • ASTM
    D5441-98(2013) Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography
    Edition: 2013
    $103.58
    Unlimited Users per year

Description of ASTM-D5441 2013

ASTM D5441-98-Reapproved2013

Historical Standard: Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography




ASTM D5441

Scope

1.1 This test method covers the determination of the purity of methyl tert-butyl ether (MTBE) by gas chromatography. It also provides a procedure to measure impurities in MTBE such as C4 to C12 olefins, methyl, isopropyl and tert-butyl alcohols, methyl sec-butyl and methyl tert-amyl ethers, acetone, and methyl ethyl ketone. Impurities are determined to a minimum concentration of 0.02 mass %.

1.2 This test method is not applicable to the determination of MTBE in gasoline.

1.3 Water cannot be determined by this test method and must be measured by a procedure such as Test Method D1364 and the result used to normalize the chromatographic values.

1.4 A majority of the impurities in MTBE is resolved by the test method, however, some co-elution is encountered.

1.5 This test method is inappropriate for impurities that boil at temperatures higher than 180°C or for impurities that cause poor or no response in a flame ionization detector, such as water.

1.6 The values stated in SI (metric) units of measurement are preferred and used throughout the standard. Alternate units, in common usage, are also provided to improve clarity and aid the user of this test method.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Keywords

methyl tert-butyl ether; MTBE; open tubular column gas chromatography


ICS Code

ICS Number Code 71.080.60 (Alcohols. Ethers)


DOI: 10.1520/D5441-98R13

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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