1. Scope

1.1 This test method covers the analysis for commonly determined trace metals in test specimens of raw and calcined petroleum coke by inductively coupled plasma atomic emission spectroscopy.

1.2 Elements for which this test method is applicable are listed in Table 1. Detection limits, sensitivity, and optimum ranges of the metals will vary with the matrices and model of spectrometer.

1.3 This test method is applicable only to samples containing less than one mass percent ash.

1.4 Elements present at concentrations above the upper limit of the working ranges can be determined with additional, appropriate dilutions.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis

D1193 Specification for Reagent Water

E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves

Keywords

aluminum; barium; calcium; elements; ICP-AES; inductively coupled plasma; iron; magnesium; manganese; metals; nickel; petroleum coke; silicon; sodium; spectrometry, atomic emission; titanium; vanadium; zinc; Calcium content--petroleum products; ICP-AES (inductively-coupled plasma atomic emission spectrometry); Iron; Magnesium content--petroleum products; Manganese content--petroleum products; Nickel content--petroleum products; Petroleum coke; Silicon content--petroleum products; Sodium content--petroleum products; Titanium (Ti)/alloys; Trace elements--petroleum products; Vanadium content--petroleum products; Zinc content--petroleum products; Aluminum content--petroleum products; Atomic emission spectrometry; Barium content--petroleum products

ICS Code

ICS Number Code 75.160.10 (Solid fuels)

DOI: 10.1520/D5600-98

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