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  • ASTM
    D5623-94(1999)e1 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection
    Edition: 1999
    $103.58
    Unlimited Users per year

Description of ASTM-D5623 1999

ASTM D5623-94-e1-Reapproved1999

Historical Standard: Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection




ASTM D5623

Scope

1.1 This test method covers the determination of volatile sulfur-containing compounds in light petroleum liquids. This test method is applicable to distillates, gasoline motor fuels (including those containing oxygenates) and other petroleum liquids with a final boiling point of approximately 230°C (450°F) or lower at atmospheric pressure. The applicable concentration range will vary to some extent depending on the nature of the sample and the instrumentation used; however, in most cases, the test method is applicable to the determination of individual sulfur species at levels of 0.1 to 100 mg/kg.

1.2 The test method does not purport to identify all individual sulfur components. Detector response to sulfur is linear and essentially equimolar for all sulfur compounds within the scope (1.1) of this test method; thus both unidentified and known individual compounds are determined. However, many sulfur compounds, for example, hydrogen sulfide and mercaptans, are reactive and their concentration in samples may change during sampling and analysis. Coincidently, the total sulfur content of samples is estimated from the sum of the individual compounds determined; however, this test method is not the preferred method for determination of total sulfur.

1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Keywords

atomic emission detection; gas chromatography; sulfur chemiluminescence detection; sulfur compounds


ICS Code

ICS Number Code 75.160.20 (Liquid fuels)


DOI: 10.1520/D5623-94R99E01

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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