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  • ASTM
    D5932-08(2013)e1 Standard Test Method for Determination of 2,4-Toluene Diisocyanate (2,4-TDI) and 2,6-Toluene Diisocyanate (2,6-TDI) in Air (with 9-(N-Methylaminomethyl) Anthracene Method) (MAMA) in the Workplace
    Edition: 2013
    $103.58
    Unlimited Users per year

Description of ASTM-D5932 2013

ASTM D5932-08-e1-Reapproved2013

Historical Standard: Standard Test Method for Determination of 2,4-Toluene Diisocyanate (2,4-TDI) and 2,6-Toluene Diisocyanate (2,6-TDI) in Air (with 9-(N-Methylaminomethyl) Anthracene Method) (MAMA) in the Workplace




ASTM D5932

Scope

1.1 This test method covers the determination of gaseous 2,4-toluene diisocyanate (2,4-TDI) and 2,6-toluene diisocyanate (2,6-TDI) in air samples collected from workplace and ambient atmospheres.

1.2 Differential air sampling is performed with a segregating device.2,3 The gaseous fraction is collected on a glass fiber filter (GFF) impregnated with 9-(N-methylaminomethyl) anthracene (MAMA).

1.3 The analysis of the gaseous fraction is performed with a high performance liquid chromatograph (HPLC) equipped with ultraviolet (UV) and fluorescence detectors.

1.4 The analysis of the aerosol fraction is performed separately as described in Ref (1).4

1.5 The range of application of this test method, utilizing UV and a fluorescence detector, is validated for 0.029 to 1.16 μg of monomer 2,4- and 2,6-TDI/2.0 mL of desorption solution, which corresponds to concentrations of 0.002 to 0.077 mg/m3 of TDI based on a 15-L air sample. This corresponds to 0.28 to 11 ppb(V) and brackets the established TLV value of 5 ppb(v).

1.6 A field blank sampling system is used to check the possibility of contamination during the entire sampling and analysis.

1.7 The values stated in SI units are to be regarded as the standard.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Keywords

air monitoring; dual filter sampling system; high-performance liquid chromatography; sampling and analysis; toluene diisocyanate; workplace atmospheres; 9-(N-methylaminomethyl) anthracene;


ICS Code

ICS Number Code 13.040.30 (Workplace atmospheres)


DOI: 10.1520/D5932-08R13E01

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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