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  • ASTM
    D7845-13 Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography – Mass Spectrometry
    Edition: 2013
    $113.57
    Unlimited Users per year

Description of ASTM-D7845 2013

ASTM D7845-13

Historical Standard: Standard Test Method for Determination of Chemical Species in Marine Fuel Oil by Multidimensional Gas Chromatography – Mass Spectrometry




ASTM D7845

Scope

1.1 This test method covers the quantitative determination of a variety of chemical species in marine fuel oil (bunker fuel oil) by gas chromatography – mass spectrometry. By using the same conditions and by selecting required mass spectral selected ions, the test method may be used for the determination of other species than those for which precision statements and limits of detection have been established.

1.2 An example list of chemical species for which a limit of quantification has been determined by means of this test method is given in Table 1.

TABLE 1 Component Table

 

Limit of Quantitation
mg/kg

n-butyl alcohol

10

Cyclohexanol

10

n-butyl ether

10

n-butyl acylate

10

Styrene

10

alpha-pinene

10

Phenol

20

alpha-methyl styrene

10

beta-pinene

10

4-methyl styrene

10

trans-B-methyl styrene

10

3-methyl styrene

10

2-methyl styrene

10

Dicyclopentadiene

10

Limonene

10

Indene

20

1-phenyl ethanol

20

para, alpha-Dimethyl styrene

20

2,5 dimethyl styrene

20

2,4 dimethyl styrene

20

2-phenyl ethanol (phenylethanol)

20

2-Ethyl Phenol

50

2,4 Dimethyl Phenol

20

4-Ethyl Phenol (co elutes with 3-ethylphenol)

20

2-Phenoxy-1-propanol

50

2-Phenoxy ethanol

50

4-isopropylphenol

50

1-Phenoxy-2-Propanol

20

Styrene Glycol

50


1.3 Other refinery hydrocarbon fractions and their mixtures may be tested using the same test method conditions. However, the precision of this test method reflects the compounds in Table 1.

1.4 Results are reported to the nearest 1.0 mg/kg.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Keywords

bunker fuel oil; gas chromatography; GC/MS; marine fuel oil; mass spectrometry


ICS Code

ICS Number Code 47.020.20 (Marine engines and propulsion systems)


DOI: 10.1520/D7845-13

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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