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  • ASTM
    D803-12 Standard Test Methods for Testing Tall Oil
    Edition: 2012
    $91.10
    Unlimited Users per year

Description of ASTM-D803 2012

ASTM D803 - 12

Standard Test Methods for Testing Tall Oil

Active Standard ASTM D803 | Developed by Subcommittee: D01.34

Book of Standards Volume: 06.03




ASTM D803

Significance and Use

3.1 Tall oil, both crude and refined, is an important by-product of the alkaline (kraft) pulping of pine wood. It consists primarily of fatty acids, resin acids, and neutral materials; the levels of these various components depend on factors such as the species of pine tree, geographic location, climate, etc.

3.1.1 Tall oil is used primarily as a commercial source of fatty acids and rosin, and, therefore, reliable methods for the analysis of these components is necessary.

1. Scope

1.1 These test methods cover the test procedures to be applied to whole tall oils or refined tall oils. Previous editions of these test methods have described test procedures that are used to test tall oil fatty acid, rosin, and other tall oil-derived products as well as test crude and refined tall oil. Consequently, these test methods are widely cited in reference books and industry literature for the testing of tall oil-derived products.

1.1.1 In this current revision, procedural details of some of the often-cited test methods have been removed and the test methods consolidated with other existing test methods. In such cases the consolidated methods, applicable to all tall oil-derived products.

1.2 The procedures appear in the following order:

Physical Tests

Sections

Viscosity:

Brookfield Method (Preferred Method)

7

Bubble Time Method

8

Flash Point

9

Color

10

Moisture:

11

Insoluble Matter

12

Ash

13

Chemical Analysis

Acid Number

16

Saponification Number

17

Rosin Acids

18

Unsaponifiable Matter

19

Fatty Acids

20


1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D92 Test Method for Flash and Fire Points by Cleveland Open Cup Tester

D93 Test Methods for Flash Point by Pensky-Martens Closed Cup Tester

D269 Test Method for Insoluble Matter in Rosin and Rosin Derivatives

D464 Test Methods for Saponification Number of Naval Store Products Including Tall Oil and Other Related Products

D465 Test Methods for Acid Number of Naval Stores Products Including Tall Oil and Other Related Products

D890 Test Method for Water in Liquid Naval Stores

D1065 Test Method for Unsaponifiable Matter in Naval Stores, Including Rosin, Tall Oil, and Related Products

D1240 Test Methods for Rosin Acids Content of Naval Stores, Including Rosin, Tall Oil, and Related Products

D1466 Test Method for Sampling Liquid Oils and Fatty Acids Commonly Used in Paints, Varnishes, and Related Materials

D1544 Test Method for Color of Transparent Liquids (Gardner Color Scale)

D1545 Test Method for Viscosity of Transparent Liquids by Bubble Time Method

D1585 Test Methods for Fatty Acids Content of Naval Stores, Including Rosin, Tall Oil, and Related Products

D2196 Test Methods for Rheological Properties of Non-Newtonian Materials by Rotational (Brookfield type) Viscometer

D3278 Test Methods for Flash Point of Liquids by Small Scale Closed-Cup Apparatus

D5974 Test Methods for Fatty and Rosin Acids in Tall Oil Fractionation Products by Capillary Gas Chromatography

D6166 Test Method for Color of Naval Stores and Related Products (Instrumental Determination of Gardner Color)

E300 Practice for Sampling Industrial Chemicals


Keywords

acid number; fatty acids; rosin acids; saponification number; tall oil;


ICS Code

ICS Number Code 87.060.20 (Binders)


DOI: 10.1520/D0803-12

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ASTM D803

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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