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  • ASTM
    E2070-13 Standard Test Method for Kinetic Parameters by Differential Scanning Calorimetry Using Isothermal Methods
    Edition: 2013
    $113.57
    Unlimited Users per year

Description of ASTM-E2070 2013

ASTM E2070-13

Historical Standard: Standard Test Method for Kinetic Parameters by Differential Scanning Calorimetry Using Isothermal Methods




ASTM E2070

Scope

1.1 Test Methods A, B, and C determine kinetic parameters for activation energy, pre-exponential factor and reaction order using differential scanning calorimetry from a series of isothermal experiments over a small ( ≈10 K) temperature range. Test Method A is applicable to low nth order reactions. Test Methods B and C are applicable to accelerating reactions such as thermoset curing or pyrotechnic reactions and crystallization transformations in the temperature range from 300 to 900 K (nominally 30 to 630°C). This test method is applicable only to these types of exothermic reactions when the thermal curves do not exhibit shoulders, double peaks, discontinuities or shifts in baseline.

1.2 Test Methods D and E also determines the activation energy of a set of time-to-event and isothermal temperature data generated by this or other procedures

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This test method is similar but not equivalent to ISO DIS 11357, Part 5, and provides more information than the ISO standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.


Keywords

activation energy; accelerating reactions; Avrami equation; crystallization reactions; differential scanning calorimetry (DSC); frequency factor; kinetics; nth order reactions; pre-exponential factor; reactions; Sestak-Berggren equation; thermal analysis; thermoset cure


ICS Code

ICS Number Code 17.200.10 (Heat. Calorimetry)


DOI: 10.1520/E2070-13

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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