1. Scope

1.1 This test method describes a laboratory procedure for conducting an electrochemical reactivation (EPR) test on AISI Type 304 and 304L (UNS No. S30400 and S30403, respectively) stainless steels. This test method can provide a nondestructive means of quantifying the degree of sensitization in these steels (1, 2, 3). This test method has found wide acceptance in studies of the effects of sensitization on intergranular corrosion and intergranular stress corrosion cracking behavior (see Terminology G15). The EPR technique has been successfully used to evaluate other stainless steels and nickel base alloys (4), but the test conditions and evaluation criteria used were modified in each case from those cited in this test method.

1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

A262 Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels

D1193 Specification for Reagent Water

E3 Guide for Preparation of Metallographic Specimens

E7 Terminology Relating to Metallography

E112 Test Methods for Determining Average Grain Size

G1 Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens

G3 Practice for Conventions Applicable to Electrochemical Measurements in Corrosion Testing

G5 Reference Test Method for Making Potentiostatic and Potentiodynamic Anodic Polarization Measurements

G15 Terminology Relating to Corrosion and Corrosion Testing

G28 Test Methods for Detecting Susceptibility to Intergranular Corrosion in Wrought, Nickel-Rich, Chromium-Bearing Alloys

G61 Test Method for Conducting Cyclic Potentiodynamic Polarization Measurements for Localized Corrosion Susceptibility of Iron-, Nickel-, or Cobalt-Based Alloys

Keywords

carbide precipitation; electrochemical reactivation (EPR) test; electrochemical test; intergranular corrosion; sensitization; stress corrosion cracking; Sensitization; Stainless steel (corrosion testing); Stress corrosion cracking (SCC); Carbide precipitation; Electrochemical measurements/testing; Electrochemical reactivation (EPR) test; EPR test; Intergranular attack (IGA); Nondestructive evaluation (NDE)--metallic materials; Potentiodynamic anodic polarization measurements;

ICS Code

ICS Number Code 77.140.20 (Steels of high quality)

DOI: 10.1520/G0108-94R99

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