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  • BSI
    BS EN 17212:2019 Animal Feeding stuffs. Methods of sampling and analysis. Determination of melamine and cyanuric acid content by liquid chromatographic method with mass spectrometric detection (LC-MS/MS)
    Edition: 2019
    $418.55
    / user per year

Description of BS EN 17212:2019 2019

This document specifies a high-performance liquid chromatographic (HPLC) mass spectrometric (MS) method for screening and quantification of melamine and cyanuric acid in the concentration range between 1 mg/kg and 100 mg/kg feed. The method is validated in an international collaborative trial for melamine in complete feed, complementary feed, feed material, milk replacer and pet food including canned pet food in the range between 1 mg/kg and 80 mg/kg with particular regard to the maximum level of 2,5 mg/kg as established by the European Commission. Laboratory experiences have shown that the method is also applicable for cyanuric acid in the same concentration range in complete feed (n = 7), complementary feed (n = 6), feed material (n = 7, resp. 9), milk replacer (n = 7) and pet food (n = 7) including canned pet food. Since the LC-MS/MS sensitivity for cyanuric acid is lower than for melamine, it has to be ensured that the LC-MS/MS system is in excellent working order. The method is applicable to feeding stuffs but not tested for pre-mixtures and feed additives. Quantification of concentrations above 100 mg/kg is possible, but the method has to be validated by the operator.

Standard NumberBS EN 17212:2019
TitleAnimal Feeding stuffs. Methods of sampling and analysis. Determination of melamine and cyanuric acid content by liquid chromatographic method with mass spectrometric detection (LC-MS/MS)
StatusDefinitive
Publication Date2019-09-12
Identical National Standard OfEN 17212
DescriptorsMass, Liquid chromatography, Determination of content, Cyanuric acid, Melamine, Analysis, Feed (animal)
ICS65.120 Animal feeding stuffs
CommitteeAW/10
ISBN978 0 580 93223 6
PublisherBSI
Pages40

About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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