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  • BSI
    BS EN 17322:2020 Environmental Solid Matrices. Determination of polychlorinated biphenyls (PCB) by gas chromatography. mass selective detection (GC-MS) or electron-capture detection (GC-ECD)
    Edition: 2020
    $489.87
    / user per year

Description of BS EN 17322:2020 2020

This document specifies methods for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in soil, sludge, sediment, treated biowaste, and waste using GC-MS and GC-ECD (see Table 2).

Table 2
Target analytes of this European Standard
Target analyte CAS-RN a
PCB28 2,4,4'-trichlorobiphenyl 7012– 37–5
PCB52 2,2',5,5'-tetrachlorobiphenyl 35693–b b b b b 99–3
PCB101 2,2',4,5,5'-pentachlorobiphenyl 37680–b b b b b 73–2
PCB118 2,3',4,4',5-pentachlorobiphenyl 31508–b b b b b 00–6
PCB138 2,2',3,4,4',5'-hexachlorobiphenyl 35065–b b b b b 28–2
PCB153 2,2',4,4',5,5'-hexachlorobiphenyl 35065–b b b b b 27–1
PCB180 2,2',3,4,4',5,5'-heptachlorobiphenyl 35065–b b b b b 29–3
a

CAS-RN Chemical Abstracts Service Registry Number.

The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract.

Under the conditions specified in this document, lower limit of application from 1 ?g/kg (expressed as dry matter) for soils, sludge and biowaste to 10 ?g/kg (expressed as dry matter) for solid waste can be achieved. For some specific samples the limit of 10 ?g/kg cannot be reached.

Sludge, waste and treated biowaste may differ in properties, as well as in the expected contamination levels of PCB and presence of interfering substances. These differences make it impossible to describe one general procedure. This document contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used.

NOTE

The analysis of PCB in insulating liquids, petroleum products, used oils and aqueous samples is referred to in EN 61619 , EN 12766?1 and EN ISO 6468 respectively.

The method can be applied to the analysis of other PCB congeners not specified in the scope, provided suitability is proven by proper in-house validation experiments.



Standard NumberBS EN 17322:2020
TitleEnvironmental Solid Matrices. Determination of polychlorinated biphenyls (PCB) by gas chromatography. mass selective detection (GC-MS) or electron-capture detection (GC-ECD)
StatusDefinitive
Publication Date2020-10-08
ReplacesBS EN 15308:2016, BS EN 16167:2018
Identical National Standard OfEN 17322:2020
CorrectsBS EN 17322:2020
DescriptorsWastes, Sludge, Soils, Chromatography, Polychlorinated biphenyls
ICS13.030.01 Wastes in general, 13.030.20 Liquid wastes. Sludge, 13.030.10 Solid wastes, 13.080.10 Chemical characteristics of soils
CommitteeEH/4
ISBN978 0 539 15649 2
PublisherBSI
Pages48

About BSI

BSI Group, also known as the British Standards Institution is the national standards body of the United Kingdom. BSI produces technical standards on a wide range of products and services and also supplies certification and standards-related services to businesses.
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