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  • ASTM
    D5227-13 Standard Test Method for Measurement of Hexane Extractable Content of Polyolefins
    Edition: 2013
    $91.10
    Unlimited Users per year

Description of ASTM-D5227 2013

ASTM D5227 - 13

Standard Test Method for Measurement of Hexane Extractable Content of Polyolefins

Active Standard ASTM D5227 | Developed by Subcommittee: D20.70

Book of Standards Volume: 08.03




ASTM D5227

Significance and Use

5.1 FDA requirements for maximum extractables are specified for resin and uses. This test method provides a means to determine the amount of hexane-soluble low molecular weight material present in polyolefins. It is applicable to resins containing greater than 0.20?% extractables.

1. Scope

1.1 This test method describes an extraction/gravimetric procedure for determination of the amount of hexane soluble low molecular weight material present in polyethylene, polypropylene, ethylene-propylene copolymers, and ethylene-vinyl acetate copolymers. This test method is a modification of the Food and Drug Administration (FDA) procedure for determining hexane extractables of polyolefins. This test method is based upon the presumption that the weight of the residue extract present in the solvent is equal to the amount extracted from the film sample and could therefore be quantified by measuring the weight loss of the extracted film, eliminating the complex and time-consuming evaporation process described in 21 CFR 177.1520.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.3 The values stated in SI units are to be regarded as the standard. Units used in 21 CFR 177.1520 are also used in this test method. Units are in conformance with Federal Code 21 CFR 177.1520, from which this test method is derived.

Note 1 There is no known ISO equivalent to this standard.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D883 Terminology Relating to Plastics

D1239 Test Method for Resistance of Plastic Films to Extraction by Chemicals

D1600 Terminology for Abbreviated Terms Relating to Plastics

E131 Terminology Relating to Molecular Spectroscopy

E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

Federal Document

21 CFR 177.1520

Keywords

ethylene-propylene copolymers; ethylene-vinyl acetate copolymers; extractables; FDA; hexane; plastics; polyethylene; solvent extraction;


ICS Code

ICS Number Code 83.080.20 (Thermoplastic materials)


DOI: 10.1520/D5227

ASTM International is a member of CrossRef.

ASTM D5227

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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